I-GDW-106 Oil Dew Point Tester
●Le miyalo elandelayo isetshenziswa umuntu oqeqeshiwe ukugwema ukushaqeka kagesi.Ungenzi noma iyiphi isevisi ngale kweziyalezo zokusebenza ngaphandle uma ufanelekile ukwenza kanjalo.
●Ungalusebenzisi lolu cingo endaweni evuthayo nemanzi.Gcina ingaphezulu lihlanzekile futhi lomile.
●Sicela uqinisekise ukuthi okokusebenza kuqondile ngaphambi kokuvula.Ungawisi okokusebenza ugweme kakhulu ukulimala kokunyakaza kwemishini.
●Beka okokusebenza endaweni eyomile, ehlanzekile, engenawo umoya oshisayo.Ukupakisha impahla ngaphandle kweziqukathi zokuthutha kuyingozi.
●Iphaneli kufanele iqonde ngesikhathi sokugcina.Phakamisa izinto ezigciniwe ukuze uzivikele emswakama.
●Ungaliqeqeshi ithuluzi ngaphandle kwemvume, okuzothinta iwaranti yomkhiqizo.Imboni ayinasibopho sokuzidiliza.
Isikhathi sewaranti salolu chungechunge unyaka OWODWA kusukela ngosuku othunyelwe ngalo, sicela ubheke i-invoyisi yakho noma amadokhumenti okuthumela ukuze unqume izinsuku ezifanelekile zesiqinisekiso.I-HVHIPOT corporation iqinisekisa kumthengi wangempela ukuthi lo mkhiqizo ngeke ungabi nasici ezintweni ezibonakalayo kanye nomsebenzi owenziwayo ngaphansi kokusetshenziswa okuvamile.Phakathi naso sonke isikhathi sewaranti, hlinzeka ngokuthi lokho kulimala akunqunywanga i-HVHIPOT ukuthi kudalwe ukuhlukumeza, ukusetshenziswa kabi, ukuguqulwa, ukufakwa okungafanele, ukunganaki noma isimo esibi semvelo, i-HVHIPOT ikhawulelwe kuphela ukulungisa noma ukushintshwa kwaleli thuluzi phakathi nenkathi yesiqinisekiso.
| Cha. | Igama | Qty. | Iyunithi |
| 1 | Umsingathi we-GDW-106 | 1 | ucezu |
| 2 | Electrolytic cell bottle | 1 | ucezu |
| 3 | Electrolytic electrode | 1 | ucezu |
| 4 | I-electrode yokulinganisa | 1 | ucezu |
| 5 | Electrolytic cell injection plug | 1 | ucezu |
| 6 | Ipulaki yokugaya ingilazi enkulu | 1 | ucezu |
| 7 | Ipulaki yokugaya ingilazi encane (notch) | 1 | ucezu |
| 8 | Ipulaki yokugaya ingilazi encane | 1 | ucezu |
| 9 | Induku enyakazayo | 2 | ama-pcs |
| 10 | Izinhlayiya ze-silica gel | 1 | isikhwama |
| 11 | I-silica gel pad | 9 | ama-pcs |
| 12 | 0.5μl isampula encane | 1 | ucezu |
| 13 | 50μl isampula encane | 1 | ucezu |
| 14 | 1 ml isampula encane | 1 | ucezu |
| 15 | Ithubhu elomile eliqondile | 1 | ucezu |
| 16 | Intambo yamandla | 1 | ucezu |
| 17 | Vacuum amafutha | 1 | ucezu |
| 18 | I-Electrolyte | 1 | Ibhodlela |
| 19 | Iphepha lokuphrinta | 1 | gingqa |
| 20 | Igayidi yomsebenzisi | 1 | ucezu |
| 21 | Umbiko wokuhlola | 1 | ucezu |
I-HV Hipot Electric Co., Ltd. iye yalihlola ngokucophelela nangokucophelela le manuwali, kodwa ngeke siqinisekise ukuthi awekho amaphutha nokushiywa ngokuphelele encwadini.
I-HV Hipot Electric Co., Ltd. izibophezele ekwenzeni ngcono okuqhubekayo emisebenzini yomkhiqizo, kanye nokwenza ngcono ikhwalithi yesevisi, ngakho inkampani ihlala inelungelo lokushintsha noma yimiphi imikhiqizo nezinhlelo zesofthiwe ezichazwe kuleli bhukwana kanye nokuqukethwe kwaleli bhukwana ngaphandle kwangaphambi kwalokho. isaziso.
Ubuchwepheshe be-Coulometric Karl Fischer busetshenziswa ukukala umswakama wokulandelela ngokunembile isampula elinganisiwe equkethe.Ubuchwepheshe busetshenziselwa kakhulu ukunemba kanye nezindleko zokuhlola ezishibhile.Imodeli ye-GDW-106 ilinganisela ngokunembile umswakama kumasampula oketshezi, aqinile negesi ngokobuchwepheshe.Isetshenziswa kugesi, kuphethiloli, kumakhemikhali, ekudleni nokunye.
Leli thuluzi lisebenzisa amayunithi okucubungula esizukulwane esisha esinamandla kanye nesekhethi entsha sha kanye nokuthi ukusetshenziswa kwamandla okuphansi okuphakeme kuyenza ikwazi ukusebenzisa ibhethri losayizi omncane futhi ephathekayo.Ukwahlulela indawo yokuphela kwe-electrolysis kusekelwe ekuhloleni isignali ye-electrode futhi ukuzinza nokunemba yizici ezibalulekile zokunemba kokuzimisela.
●5-intshi high-definition umbala wesikrini esithintwayo, isibonisi sicacile futhi kulula ukusebenza.
●Izindlela ezimbili zesinxephezelo samanje esingenalutho se-electrolyte kanye nesinxephezelo sokudonswa kwebhalansi ukuze kubuyekezwe imiphumela yokuhlola.
●Imisebenzi yokuthola iphutha lesifunda sokulinganisa i-electrode kanye nephutha lesekethe emfushane.
●Yamukela iphrinta encane eshisayo, ukuphrinta kulula futhi kuyashesha.
●5 amafomula wokubala akhiwe ensimbini, futhi iyunithi yokubala yemiphumela yokuhlolwa (mg / L, ppm%) ingakhethwa njengoba kudingekile.
●Londoloza ngokuzenzakalelayo amarekhodi omlando ngethebhu yesikhathi, umkhawulo ufike kumarekhodi angu-500.
●I-microprocessor yamanje engenalutho ilawula ngokuzenzakalelayo isinxephezelo, futhi ama-reagents angafinyelela ukulingana ngokushesha.
●Ibanga Lokulinganisa: 0ug-100mg;
●Ukunemba kokulinganisa:
Electrolysis amanzi Ukunemba
3ug-1000ug ≤±2ug
>1000ug ≤±02% (amapharamitha angenhla awafaki iphutha lomjovo)
●Isixazululo: 0.1ug;
●I-Electrolyzing Yamanje: 0-400mA;
●Ukusetshenziswa kwamandla okuphezulu: 20W;
●Okokufaka Amandla: AC230V±20%, 50Hz±10%;
●Izinga lokushisa elisebenzayo le-Ambient: 5～40℃;
●Umswakamo we-Ambient osebenzayo: ≤85%
●Ubukhulu: 330×240×160mm
●Isisindo Net: 6kg.
Ukwakheka Nezinsimbi
1. Umsingathi
Umfanekiso 4-1 Umsingathi
2. Iseli Electrolytic
Umfanekiso 4-2 Umdwebo we-Electrolytic cell decomposition
Umfanekiso 4-3 Umdwebo womhlangano weseli we-Electrolytic
1.I-electrode yokulinganisa 2. I-electrode lead lead 3. Electrolytic electrode 4. Electrolytic electrode lead 5. Ion filter membrane 6. Ukomisa ipulaki yokugaya ingilazi yeshubhu 7. Ishubhu yokomisa 8. I-allochroic silicagel (i-drying agent) 9. Isampula yokungena 10. Stirre Igumbi le-anode 12. Igumbi le-Cathode 13. Ipulaki yokugaya ingilazi yeseli ye-Electrolytic
●Faka izinhlayiya ze-silicone ezihlaza okwesibhakabhaka (i-ejenti yokomisa) epayipini lokumisa (7 ku-Fig. 4-2).
Qaphela: Ipayipi le-tube yokomisa kufanele igcine umoya othile wokungena futhi ayikwazi ukuvalwa ngokuphelele, ngaphandle kwalokho kulula ukubangela ingozi!
●Faka iphedi ye-silicone emhlophe e-milky eqhude futhi uyijike ngokulinganayo ngezigxobo zokubopha (bheka umdwebo 4-4).
Umfanekiso 4-4 Umdwebo wokuhlanganisa ipulaki lomjovo
●Faka ngokucophelela isivusi ebhodleleni le-electrolytic ngomnyango wesampula.
●Sabalalisa ngokulinganayo ungqimba lwamafutha e-vacuum ku-electrode yokulinganisa, i-electrolytic electrode, ishubhu yokomisa yegumbi le-cathode, kanye nembobo yokugaya iqhude elingenisayo.Ngemva kokufaka izingxenye ezingenhla ebhodleleni le-electrolytic, liphendukise ngobumnene ukuze livaleke kangcono.
●Cishe i-120-150 ml ye-electrolyte ijova egunjini le-anode yeseli ye-electrolytic isuka embobeni yokuvala iseli ye-electrolytic ngefaneli ehlanzekile neyomile (noma kusetshenziswa isishintshi esiwuketshezi), iphinde ijovelwe egumbini le-anode leseli le-electrolytic lisuka Imbobo yokuvala i-electrolytic electrode ngefaneli (noma kusetshenziswa isiguquli esiwuketshezi), ukwenza izinga le-electrolyte ngaphakathi kwegumbi le-cathode negumbi le-anode liyafana ngokuyisisekelo.Ngemva kokuphothula, ipulaki yokugaya ingilazi yeseli ye-electrolytic imbozwe ngokulinganayo ngesendlalelo se-vacuum grease futhi ifakwe endaweni ehambisanayo, ijikelezwe ngobumnene ukuze ivalwe kangcono.
Qaphela: Umsebenzi ongenhla wokulayisha i-electrolyte kufanele wenziwe endaweni enomoya omuhle.Ungahogeli noma uthinte ama-reagents ngesandla.Uma ithinta esikhumbeni, yigeze ngamanzi.
Ngemva kokuqeda lezi zinyathelo ezingenhla, faka ingqamuzana ye-electrolytic kusekelo lweseli ye-electrolytic (9 kuFig. 4-1), faka intambo yokuxhuma i-electrolytic electrode nepulaki ye-lotus kanye nentambo yokulinganisa i-electrode kusixhumi esibonakalayo se-electrode electrode ( 7 kuFig. . 4-1).) kanye ne-electrode interface yokulinganisa (8 ku-Fig.4-1).
Isixazululo se-reagent siyingxube ye-iodine, i-pyridine egcwele isulfure dioxide ne-methanol.Isimiso sokusabela se-Karl-Fischer reagent ngamanzi siwukuthi: ngokusekelwe ebukhoneni bamanzi, i-iodine iyancipha nge-sulfur dioxide, futhi phambi kwe-pyridine ne-methanol, i-pyridine hydroiodide ne-methyl hydrogen hydrogen pyridine kwakhiwa.Ifomula yokusabela ithi:
H20+I2+SO2+3C5H5N → 2C5H5N·HI+C5H5N·SO3 …………(1)
C5H5N·SO3+CH3OH → C5H5N·HSO4CH3 ……………………(2)
Ngesikhathi senqubo ye-electrolysis, ukusabela kwe-electrode imi kanje:
I-Anode: 2I- - 2e → I2 ..........................................(3)
I-Cathode: 2H+ + 2e → H2↑..............................................(4)
I-iodine ekhiqizwe i-anode isabela emanzini ukuze yakhe i-hydroiodic acid kuze kube yilapho kuqedwa ukusabela kwawo wonke amanzi, futhi ukuphela kokusabela kuboniswa iyunithi yokubona eyakhiwe ipheya lama-electrode eplatinamu.Ngokomthetho kaFaraday we-electrolysis, inani lama-athomu e-iodine abamba iqhaza ekuphenduleni lilingana nenani lama-molecule amanzi, elilingana nenani lokushaja kagesi.Inani lamanzi nokushaja kunezibalo ezilandelayo:
W=Q/10.722 ………………………………………………(5)
W--okuqukethwe komswakama weyunithi yesampula: ug
Q--inani le-electrolysis yeyunithi yokushaja kagesi: mC
Ithuluzi lamukela i-LCD yesikrini esikhulu, futhi inani lolwazi elingaboniswa esikrinini ngasinye licebile, okunciphisa inani lokushintsha izikrini.Ngezinkinobho zokuthinta, imisebenzi yezinkinobho ichazwe ngokucacile, kulula ukuyisebenzisa.
Insimbi ihlukaniswe ngezikrini ezi-5 zokubonisa:
●Isikrini sokwamukela i-boot;
●Isikrini sokusetha isikhathi;
●Isikrini sedatha yomlando;
●Isikrini sokuhlola isampula;
●Isikrini somphumela wokulinganisa;
1. Isikrini Sokwamukela Sokuqalisa
Xhuma intambo yamandla wensimbi bese uvula iswishi yamandla.Isikrini se-LCD sibonisa njengoba kukhonjisiwe kuMfanekiso 6-1:
2.Time Setting Screen
Cindezela inkinobho ethi "Isikhathi" kusixhumi esibonakalayo soMfanekiso 6-1, futhi isikrini se-LCD sizovela njengoba kukhonjisiwe kuMfanekiso 6-2:
Kulesi sixhumi esibonakalayo, cindezela ingxenye yezinombolo yesikhathi noma idethi amasekhondi angu-3 ukuze usethe noma ulinganise isikhathi nosuku.
Cindezela
ukhiye wokubuyela ku-boot interface.
3. Isikrini Sedatha Yomlando
Cindezela inkinobho ethi "Idatha" esikrinini soMfanekiso 6-1, futhi isikrini se-LCD sizovela njengoba kukhonjisiwe kuMfanekiso 6-3:
Cindezela
ukhiye wokushintsha amakhasi.
Cindezela
Ukhiye wokususa idatha yamanje.
Cindezela
ukhiye wokuphrinta idatha yamanje.
Cindezelaukhiye wokubuyela ku-boot interface.
4. Isikrini Sokuhlola Isampula
Cindezela inkinobho ethi "Hlola" esikrinini soMfanekiso 6-1, isikrini se-LCD sizovela njengoba kukhonjisiwe ngezansi:
Uma i-electrolyte kuseli ye-electrolytic isanda kushintshwa, isimo samanje sizobonisa "I-Reagent phezu kwe-iodine, sicela ugcwalise ngamanzi".Ngemva kokujova amanzi kancane kancane egunjini le-anode ngesampler engu-50ul kuze kube yilapho i-electrolyte iba phuzi ngokuphaphathekile, isimo samanje sizobonisa "Sicela ulinde", futhi ithuluzi lizobhalansisa ngokuzenzakalelayo.
Uma i-electrolyte kuseli ye-electrolytic isetshenzisiwe, isimo samanje sizobonisa "Sicela ulinde", futhi ithuluzi lizobhalansa ngokuzenzakalelayo.
I-pre-conditioning iqala, okungukuthi umkhumbi we-titration awusomisiwe."Sicela ulinde" kuzovezwa, insimbi inyakazisa amanzi engeziwe.
Cindezela
Ukhiye wokukhetha izinto.
Cindezela
Ukhiye wokuqala ukuhlolwa.
Cindezelaukhiye wokubuyela ku-boot interface
4.1 Kulesi sixhumi esibonakalayo, cindezela ukhiye othi "Setha", setha isivinini sokunyakazisa kanye no-Ext.isikhathi.
Umfanekiso 6-5
Chofoza isivinini esishukumisayo (ingxenye yenombolo) ukuze usethe isivinini esinyakazayo sensimbi.Chofoza okuthi Ext.isikhathi (ingxenye yenombolo) yokusetha isikhathi sokulibaziseka sephoyinti lokugcina lokuhlolwa.
Isivinini esishukumisayo: Uma i-viscosity yesampula ehloliwe inkulu, isivinini esishukumisayo singakhushulwa ngendlela efanele.Kungaphansi kokungabikho kwamabhamuza ku-electrolyte enyakazayo.
Ext.Isikhathi: Uma kudingekile ukunweba isikhathi sokuhlola sesampula, njengokungancibiliki kahle kwesampula kanye ne-electrolyte noma okuqukethwe kwamanzi okuhlola kwegesi, isikhathi sokuhlola singanwetshwa ngokufanelekile.(Qaphela: Uma isikhathi se-Ext. sisethelwe kumaminithi angu-0, ukuhlolwa kuqedwa ngemva kokuba ijubane le-electrolysis lensimbi lizinzile. Uma isikhathi se-Ext. sisethelwe kumaminithi angu-5, ukuhlolwa kuqhutshwa imizuzu engu-5 ngemva kwesivinini se-electrolysis insimbi izinzile)
4.2 Ngemva kokuqedwa kwebhalansi yensimbi, isimo samanje sizobonisa "Cindezelaukhiye wokulinganisa". Ngalesi sikhathi, ithuluzi lingalinganiswa noma isampula lingalinganiswa ngokuqondile.
Ukuze ulinganise ithuluzi, sebenzisa isampula engu-0.5ul ukuze uthathe u-0.1ul wamanzi, cindezela ukhiye othi "Qala", futhi uwujove ku-electrolyte ngokusebenzisa isampula yokungena.Uma umphumela wokugcina wokuhlola uphakathi kuka-97-103ug (isampulu engenisiwe), ufakazela ukuthi ithuluzi lisesimweni esivamile futhi isampula ingalinganiswa.(Umphumela wokuhlola wesampula yasekhaya uphakathi kuka-90-110ug, okufakazela ukuthi ithuluzi lisesimweni esivamile).
4.3 Isampula Lokubhalwa Kwegama
Uma insimbi ibhalansisiwe (noma ilinganisiwe), isimo samanje sithi "I-Titrating", isampuli ingalinganiswa.
Thatha inani elifanele lesampula, cindezela ukhiye "Qala", faka isampula ku-electrolyte ngokusebenzisa isampula yokufaka, futhi ithuluzi lizohlola ngokuzenzakalelayo kuze kube sekupheleni.
Qaphela: Ivolumu yesampula yehliswa ngokufanelekile noma inyuswe ngokuya ngesilinganiso samanzi sokuqukethwe kwesampula.Inani elincane lesampula lingathathwa nesampula engu-50ul ukuze lihlolwe.Uma inani lokuqukethwe kwamanzi elilinganisiwe lilincane, umthamo womjovo ungandiswa ngokufanelekile;Uma inani lokuqukethwe kwamanzi elilinganisiwe likhulu, umthamo womjovo ungancishiswa ngendlela efanele.Kuyafaneleka ukugcina umphumela wokugcina wokuhlola wokuqukethwe kwamanzi phakathi kwamashumi ama-micrograms namakhulu ama-micrograms.Uwoyela we-Transformer kanye nowoyela we-steam turbine angajovwa ngokuqondile i-1000ul.
5. Imiphumela Yesilinganiso
Ngemva kokuqedwa kokuhlolwa kwesampula, ifomula yokubala ingashintshwa njengoba kudingekile, futhi inombolo engakwesokudla kwefomula yokubala ingashintshwa ibe phakathi kuka-1-5.(ihambisana ne-ppm, mg/L kanye no-% ngokulandelana)
Ububanzi obujwayelekile bokulinganisa baleli thuluzi ngu-0μg-100mg.Ukuze kutholwe imiphumela yokuhlola enembile, inani lesampula elijovwe kufanele lilawulwe ngendlela efanele ngokokuqukethwe komswakama kwesampula yokuhlola.
1. Isampula yoketshezi
Ukukalwa kwesampula yoketshezi: isampula elihloliwe kufanele likhishwe ngomjovo wesampula, bese lijovwa egunjini le-anode leseli le-electrolytic ngokusebenzisa imbobo yomjovo.Ngaphambi komjovo wesampula, inaliti kufanele ihlanzwe ngephepha lokuhlunga.Futhi ithiphu yenaliti kufanele ifakwe ku-electrolyte ngaphandle kokuxhumana ne-inwall yeseli ye-electrolytic kanye ne-electrode lapho isampula yokuhlola ijovwa.
2. Isampula eliqinile
Isampula eliqinile lingaba ngendlela kafulawa, izinhlayiya noma i-block mess (inqwaba yebhlokhi kumele icutshungulwe).I-evaporator yamanzi efanelekile izokhethwa futhi ixhunywe ethuluzini lapho isampula yokuhlola kunzima ukuncibilika ku-reagent.
Ukuthatha isampula eliqinile elingancibilika ku-reagent njengesibonelo ukuchaza umjovo wesampula oqinile, kanje:
Umfanekiso 7-1
1) Umjovo wesampula oqinile ukhonjiswa njengomfanekiso 7-1, uwuhlanze ngamanzi bese uwomisa kahle.
2) Yehlisa isivalo somjovo wesampula oqinile, jova isampula yokuhlola, vala isembozo bese ukala ngokunembile.
3) Yehlisa ipulaki yembobo yomjovo wesampula yesampula ye-electrolytic, faka isampula lomjovo embobeni yomjovo ngokuya ngomugqa ogcwele oboniswe njengomfanekiso 7-2.Zungezisa isampula eqinile yokujova ngamadigri angu-180 aboniswe njengomugqa onachashazi kumfanekiso 7-2, okwenza isampula yokuhlola yehle ku-reagent kuze kuphele ukukalwa.Enqubeni yakho, isampula yokuhlola eqinile ayikwazi ukuthintwa nge-electrode ye-electrolytic kanye ne-electrode elinganisiwe.
Umfanekiso 7-2
Kala umjovo wesampula nesivalo ngokunembile futhi ngemva kokujova.Ikhwalithi yesampula ingabalwa ngokomehluko phakathi kwezisindo ezimbili, ezingasetshenziswa ukubala isilinganiso sokuqukethwe kwamanzi.
3. Isampula yegesi
Ukuze umswakama kugesi umuncwe i-reagent, isixhumi sizosetshenziswa ukulawula isampula yokuhlola ezofakwa kuseli ye-electrolytic noma kunini.(bona umfanekiso 7-3).Uma kulinganiswa umswakama kusampula yokuhlola igesi, i-reagent engaba ngu-150ml kufanele ijovwe kuseli ye-electrolytic ukuze kuqinisekiswe ukuthi umswakama ungamuncwa ngokugcwele.Ngesikhathi esifanayo, isivinini sokugeleza kwegesi kufanele ilawulwe ku-500ml ngomzuzu.cishe.Uma kwenzeka ukuthi i-reagent inciphisa ngokusobala ohlelweni lokulinganisa, cishe i-20ml glycol kufanele ijovwe njengesengezo.(enye i-reagent yamakhemikhali ingangezwa njengesampula langempela elilinganisiwe.)
Umfanekiso 7-3
A. Isitoreji
1. Gcina kude nokukhanya kwelanga, futhi izinga lokushisa legumbi kufanele libe phakathi kuka-5℃～35℃.
2. Ungawufaki futhi uwusebenzise ngaphansi kwemvelo enomswakama ophezulu kanye nokuguquguquka okukhulu kwamandla kagesi.
3. Ungawubeki futhi uwusebenzise ngaphansi kwemvelo enegesi ebolayo.
B. Ukushintshwa kwephedi ye-silicone
Iphedi ye-silicone embobeni yomjovo wesampula kufanele ishintshwe ngesikhathi ngenxa yokuthi ukusetshenziswa kwayo isikhathi eside kuzokwenza imbobo yephinifa ingabi yi-contractile futhi kuvumele umswakama ungene, okuzoba nomthelela esilinganisweni.(bona umfanekiso 4-4)
1. Ukushintshwa kwe-silicagel ye-allochroic
I-silicagel ye-allochroic epayipini lokomisa kufanele ishintshwe lapho umbala wayo uphenduka uluhlaza okwesibhakabhaka ngokukhanyayo usuka koluhlaza okwesibhakabhaka.Ungabeki i-silicagel powder epayipini elomisayo lapho ushintsha, ngaphandle kwalokho ukukhishwa kweseli ye-electrolytic kuzovinjelwa okuholela ekunqanyulweni kwe-electrolysis.
2. Ukugcinwa kwe-electrolytic cell polishing port
Zungezisa imbobo yokupholisha yeseli ye-electrolytic njalo ezinsukwini eziyi-7-8.Uma ingakwazi ukuphendukiswa kalula, yigcobe nge-vacuum grease ibe mncane bese uyifaka futhi, ngaphandle kwalokho kuba nzima ukuyiqaqa uma amahora esevisi made kakhulu.
Uma i-electrode ingeke yehliswe, sicela ungayikhiphi ngenkani.Ngalesi sikhathi, cwilisa lonke iseli electrolytic emanzini afudumele amahora 24-48 njalo, bese ukuyisebenzisa.
3. Ukuhlanzwa kweseli ye-electrolytic
Vula lonke unqenqema lwebhodlela lengilazi leseli ye-electrolytic.Hlanza ibhodlela leseli le-electrolytic, ipayipi elomisa, ipulaki elivala amanzi.Yomise kuhhavini(izinga lokushisa likahhavini licishe libe ngu-80 ℃) ngemva kokuhlanza, bese lipholisa ngokwemvelo.I-Absolute ethyl alcohol ingasetshenziswa ukuhlanza i-electrolusis electrode, kuyilapho amanzi enqatshelwe.Ngemuva kokuhlanza, yomise nge-dryer.
Qaphela: Ungawahlanzi ama-electrode, njengoba kubonisiwe umfanekiso 8-1
Umfanekiso 8-1
C. Faka esikhundleni i-Electrolyte
1. Thatha i-electrode electrolytic, i-electrode yokulinganisa, ishubhu yokomisa, ipulaki lomjovo nezinye izesekeli ebhodleleni leseli le-electrolytic.
2. Khipha i-electrolyte ezoshintshwa ebhodleleni leseli le-electrolytic.
3. Hlanza ibhodlela leseli le-electrolytic, i-electrolytic electrode kanye ne-electrode yokulinganisa nge-ethanol ephelele.
4. Yomisa ibhodlela leseli le-electrolytic elihlanziwe, i-electrolytic electrode, njll. kuhhavini ongekho ngaphezu kuka-50℃.
5. Thela i-electrolyte entsha ebhodleleni leseli ye-electrolytic, bese uthela inani elingaba ngu-150ml (phakathi kwemigqa emibili evundlile emhlophe yebhodlela leseli le-electrolytic).
6. Faka i-electrode ye-electrolytic, i-electrode yokulinganisa, nepulaki yesampula yeshubhu elomile, njll., bese uthela i-electrolyte entsha ku-electrolide ye-electrolytic, inani elithelwayo lilingana nezinga loketshezi lwe-electrolyte ebhodleleni leseli le-electrolytic.
7. Faka ungqimba lwamafutha evacuum kuzo zonke izimbobo zokugaya zeseli ye-electrolytic (i-electrolytic electrode, i-electrode yokulinganisa, ipulaki lomjovo, ipulaki yokugaya ingilazi).
8. Faka esikhundleni ibhodlela leseli le-electrolytic esitokisini sebhodlela leseli le-electrolytic lensimbi, bese uphendulela ithuluzi esimweni sokutsikishwa.
9. I-reagent entsha kufanele ibe nsundu ngokubomvu futhi ibe sesimweni se-iodine.Sebenzisa umjovo ongu-50uL ukujova cishe u-50-100uL wamanzi kuze kube yilapho isisebenzi siphenduka sibephuzi ngokuphaphathekile.
1. Akukho mbukiso
Imbangela: Ikhebula lamandla alixhunyiwe;inkinobho yamandla ayixhumene kahle.
Ukwelashwa: Xhuma intambo kagesi;buyisela inkinobho yamandla.
2. Vula isifunda sokulinganisa i-electrode
Imbangela: I-electrode yokulinganisa kanye nepulaki yensimbi akuxhunyiwe kahle;intambo yokuxhuma iphukile.
Ukwelashwa: Xhuma ipulaki;buyisela ikhebula.
3. I-Electrolysis velocity ihlale iyiziro ngesikhathi se-electrolysis.
Imbangela: I-electrolytic electrode kanye nepulaki yensimbi akuxhunyiwe kahle;intambo yokuxhuma iphukile.
Ukwelashwa: Xhuma ipulaki;buyisela ikhebula.
4. Umphumela wokulinganisa wamanzi ahlanzekile mancane, lapho isampula yokuhlola ijovwa, ayikwazi ukutholwa ngethuluzi.
Imbangela: I-electrolyte ilahlekelwa ukusebenza kahle.
Ukwelashwa: Faka esikhundleni se-electrolyte entsha.
5. Inqubo ye-Electrolytic ayikwazi ukuphela.
Imbangela: I-electrolyte ilahlekelwa ukusebenza kahle.
Ukwelashwa: Faka esikhundleni se-electrolyte entsha.
